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CIF Information Card
Information card for 1100748
1100747 << 1100748 >> 1100749Preview
|
Coordinates |
1100748.cif |
Structure parameters
| Formula | - C54 H70.16 Cl2 Co4 N12 O27.08 - |
| Calculated formula | - C54 H48 Cl2 Co4 N12 O27.08 - |
| Title of publication | The First Cobalt Metallacrowns: Preparation and Characterization of Mixed-Valence Cobalt(II/III), Inverse 12-Metallacrown-4 Complexes |
| Authors of publication | Theocharis C. Stamatatos; Stavroula Dionyssopoulou; Georgios Efthymiou; Panayotis Kyritsis; Catherine P. Raptopoulou; Aris Terzis; Ramon Vicente; Albert Escuer; Spyros P. Perlepes |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 3374 - 3376 |
| a | 10.523 ± 0.005 Å |
| b | 13.556 ± 0.005 Å |
| c | 12.465 ± 0.005 Å |
| α | 110.15 ± 0.01° |
| β | 95.25 ± 0.02° |
| γ | 92.05 ± 0.02° |
| Cell volume | 1658 ± 1.2 Å3 |
| Cell temperature | 298 K |
| Ambient diffraction temperature | 298 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0785 |
| Residual factor for observed reflections | 0.0596 |
| Weighted residual factors for all reflections | 0.1696 |
| Weighted residual factors for the observed reflections | 0.1546 |
| Goodness-of-fit parameter for all reflections | 1.093 |
| Goodness-of-fit parameter for observed reflections | 1.136 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |