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CIF Information Card
Information card for 1100983
1100982 << 1100983 >> 1100984Preview
|
Coordinates |
1100983.cif |
Structure parameters
| Formula | - C43.33 H51.33 B2.67 Cl2.67 F16.67 N2 O2 Pd - |
| Calculated formula | - C43.3333 H51.3333 B2.66667 Cl2.66667 F16.6667 N2 O2 Pd - |
| Title of publication | Structural Characterization of Four Members of the Electron-Transfer Series [PdII(L)2)2]n (L = o-Iminophenolate Derivative; n= 2-, 1-, 0, 1+, 2+). Ligand Mixed Valency in the Monocation and Monoanion with S=1/2 Ground States |
| Authors of publication | Swarnalatha Kokatam; Thomas Weyhermüller; Eberhard Bothe; Phalguni Chaudhuri; Karl Wieghardt |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 3709 - 3717 |
| a | 13.5833 ± 0.0005 Å |
| b | 16.8101 ± 0.0007 Å |
| c | 18.3743 ± 0.0007 Å |
| α | 78.548 ± 0.005° |
| β | 72.946 ± 0.005° |
| γ | 78.209 ± 0.005° |
| Cell volume | 3883.1 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 8 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0675 |
| Residual factor for observed reflections | 0.0568 |
| Weighted residual factors for the observed reflections | 0.1331 |
| Weighted residual factors for all reflections included in the refinement | 0.1401 |
| Goodness-of-fit parameter for observed reflections | 1.128 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |