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CIF Information Card
Information card for 1100984
1100983 << 1100984 >> 1100985Preview
|
Coordinates |
1100984.cif |
Structure parameters
| Formula | - C44 H52 Cl6 F6 N2 Ni O10 - |
| Calculated formula | - C44 H52 Cl6 F6 N2 Ni O10 - |
| Title of publication | Structural Characterization of Four Members of the Electron-Transfer Series [PdII(L)2)2]n (L = o-Iminophenolate Derivative; n= 2-, 1-, 0, 1+, 2+). Ligand Mixed Valency in the Monocation and Monoanion with S=1/2 Ground States |
| Authors of publication | Swarnalatha Kokatam; Thomas Weyhermüller; Eberhard Bothe; Phalguni Chaudhuri; Karl Wieghardt |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 3709 - 3717 |
| a | 12.8217 ± 0.0003 Å |
| b | 15.1119 ± 0.0003 Å |
| c | 13.2926 ± 0.0003 Å |
| α | 90° |
| β | 98.21 ± 0.005° |
| γ | 90° |
| Cell volume | 2549.18 ± 0.1 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Hermann-Mauguin symmetry space group | P 1 21/n 1 |
| Hall symmetry space group | -P 2yn |
| Residual factor for all reflections | 0.0592 |
| Residual factor for observed reflections | 0.0423 |
| Weighted residual factors for the observed reflections | 0.0984 |
| Weighted residual factors for all reflections included in the refinement | 0.1071 |
| Goodness-of-fit parameter for observed reflections | 1.029 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |