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CIF Information Card
Information card for 2000024
2000023 << 2000024 >> 2000025Preview
|
Coordinates |
2000024.cif |
Structure parameters
| Formula | - C24 H66 N6 S8 W6 - |
| Calculated formula | - C24 H66 N6 S8 W6 - |
| Title of publication | Ligand Substitution Reactions of W6S8L6 with Tricyclohexylphosphine (L = 4-tert-Butylpyridine or n-Butylamine): 31P NMR and Structural Studies of W6S8(PCy3)n(4-tert-butylpyridine)6-n (0 < n <= 6) Complexes |
| Authors of publication | Song Jin; D. Venkataraman; Francis J. DiSalvo |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2000 |
| Journal volume | 39 |
| Pages of publication | 2747 - 2757 |
| a | 10.0667 ± 0.0011 Å |
| b | 17.699 ± 0.002 Å |
| c | 14.374 ± 0.002 Å |
| α | 90° |
| β | 105.171 ± 0.002° |
| γ | 90° |
| Cell volume | 2471.77 Å3 |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | C 1 2/m 1 |
| Hall symmetry space group | -C 2y |
| Residual factor for all reflections | 0.154 |
| Residual factor for observed reflections | 0.0768 |
| Weighted residual factors for all reflections | 0.2482 |
| Weighted residual factors for the observed reflections | 0.0768 |
| Goodness-of-fit parameter for all reflections | 1.092 |
| Goodness-of-fit parameter for observed reflections | 1.211 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |