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CIF Information Card
Information card for 2015294
2015293 << 2015294 >> 2015295Preview
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Coordinates |
2015294.cif |
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Original IUCr paper |
HTML |
Structure parameters
| Chemical name | racemic cis-(2,2'-bipyridyl-\k^2^N,N')oxo(pentane-2,4-dionato- \k^2^O,O')(thiocyanato-\kN)vanadium(IV) |
| Formula | - C16 H15 N3 O3 S V - |
| Calculated formula | - C16 H15 N3 O3 S V - |
| Title of publication | Hydrogen-bonded sheets in racemic <i>cis</i>-(2,2'-bipyridyl-κ^2^<i>N</i>,<i>N</i>')oxo(pentane-2,4-dionato- κ^2^<i>O</i>,<i>O</i>')(thiocyanato-κ<i>N</i>)vanadium(IV) |
| Authors of publication | Kavitha, Savaridasson Jose; Panchanatheswaran, Krishnaswamy; Low, John N.; Glidewell, Christopher |
| Journal of publication | Acta Crystallographica, Section C |
| Year of publication | 2006 |
| Journal volume | 62 |
| Journal issue | 5 |
| Pages of publication | m177 - m179 |
| a | 15.0522 ± 0.001 Å |
| b | 29.721 ± 0.002 Å |
| c | 15.3753 ± 0.001 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 6878.4 ± 0.8 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | P b c a |
| Hall symmetry space group | -P 2ac 2ab |
| Residual factor for all reflections | 0.0806 |
| Residual factor for observed reflections | 0.0526 |
| Weighted residual factors for the observed reflections | 0.1237 |
| Weighted residual factors for all reflections included in the refinement | 0.135 |
| Goodness-of-fit parameter for observed reflections | 1.126 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |