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CIF Information Card
Information card for 4114558
4114557 << 4114558 >> 4114559Preview
|
Coordinates |
4114558.cif |
Structure parameters
| Formula | - C32 H51 B3 O6 Ru2 - |
| Calculated formula | - C32 H51 B3 O6 Ru2 - |
| Title of publication | Ruthenacarboranes from the Reaction of nido-1,2-(Cp*RuH)2B3H7with HC\τbCCO2Me, Cp* = η5-C5Me5. Hydrometalation, Alkyne Incorporation, and Functional Group Modification via Cooperative Metal-Boron Interactions within a Metallaborane Cluster Framework |
| Authors of publication | Hong Yan; Alicia M. Beatty; Thomas P. Fehlner |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2003 |
| Journal volume | 125 |
| Pages of publication | 16367 - 16382 |
| a | 8.799 ± 0.0004 Å |
| b | 13.0672 ± 0.0006 Å |
| c | 15.6891 ± 0.0007 Å |
| α | 101.362 ± 0.001° |
| β | 100.442 ± 0.001° |
| γ | 101.297 ± 0.001° |
| Cell volume | 1688.34 ± 0.13 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.025 |
| Residual factor for observed reflections | 0.0231 |
| Weighted residual factors for the observed reflections | 0.0591 |
| Weighted residual factors for all reflections included in the refinement | 0.0602 |
| Goodness-of-fit parameter for observed reflections | 1.064 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |