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CIF Information Card
Information card for 4114559
4114558 << 4114559 >> 4114560Preview
|
Coordinates |
4114559.cif |
Structure parameters
| Formula | - C24 H42 B2 O Ru2 - |
| Calculated formula | - C24 H42 B2 O Ru2 - |
| Title of publication | Ruthenacarboranes from the Reaction of nido-1,2-(Cp*RuH)2B3H7with HC\τbCCO2Me, Cp* = η5-C5Me5. Hydrometalation, Alkyne Incorporation, and Functional Group Modification via Cooperative Metal-Boron Interactions within a Metallaborane Cluster Framework |
| Authors of publication | Hong Yan; Alicia M. Beatty; Thomas P. Fehlner |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2003 |
| Journal volume | 125 |
| Pages of publication | 16367 - 16382 |
| a | 8.3722 ± 0.0004 Å |
| b | 19.8606 ± 0.0008 Å |
| c | 15.1043 ± 0.0006 Å |
| α | 90° |
| β | 95.638 ± 0.001° |
| γ | 90° |
| Cell volume | 2499.35 ± 0.19 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P 1 21/n 1 |
| Hall symmetry space group | -P 2yn |
| Residual factor for all reflections | 0.0278 |
| Residual factor for observed reflections | 0.0269 |
| Weighted residual factors for the observed reflections | 0.0644 |
| Weighted residual factors for all reflections included in the refinement | 0.0649 |
| Goodness-of-fit parameter for observed reflections | 1.162 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |