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CIF Information Card
Information card for 4114562
4114561 << 4114562 >> 4114563Preview
|
Coordinates |
4114562.cif |
Structure parameters
| Formula | - C60 H94 K2 O16 Si2 - |
| Calculated formula | - C60 H94 K2 O16 Si2 - |
| Title of publication | Structure and Chemistry of 1-Silafluorenyl Dianion, Its Derivatives, and an Organosilicon Diradical Dianion |
| Authors of publication | Yuxia Liu; Thomas C. Stringfellow; David Ballweg; Ilia A. Guzei; Robert West |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2002 |
| Journal volume | 124 |
| Pages of publication | 49 - 57 |
| a | 9.499 ± 0.003 Å |
| b | 12.856 ± 0.004 Å |
| c | 14.846 ± 0.004 Å |
| α | 72.274 ± 0.004° |
| β | 76.17 ± 0.005° |
| γ | 68.932 ± 0.004° |
| Cell volume | 1594.3 ± 0.8 Å3 |
| Cell temperature | 133 ± 2 K |
| Ambient diffraction temperature | 133 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.104 |
| Residual factor for observed reflections | 0.0703 |
| Weighted residual factors for the observed reflections | 0.1722 |
| Weighted residual factors for all reflections included in the refinement | 0.1946 |
| Goodness-of-fit parameter for observed reflections | 1.071 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |