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CIF Information Card
Information card for 4114686
4114685 << 4114686 >> 4114687Preview
|
Coordinates |
4114686.cif |
Structure parameters
| Chemical name | (K-2,2,2-crypt)2[Ge9(BiPh2)2].en |
| Formula | - C62 H100 Bi2 Ge9 K2 N6 O12 - |
| Calculated formula | - C62 H100 Bi2 Ge9 K2 N6 O12 - |
| Title of publication | [Ph2Bi-(Ge9)-BiPh2]2-: A Deltahedral Zintl Ion Functionalized by Exo-Bonded Ligands |
| Authors of publication | Angel Ugrinov; Slavi C. Sevov |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2002 |
| Journal volume | 124 |
| Pages of publication | 2442 - 2443 |
| a | 13.5216 ± 0.0009 Å |
| b | 13.6028 ± 0.0009 Å |
| c | 24.4984 ± 0.0017 Å |
| α | 79.7 ± 0.001° |
| β | 77.003 ± 0.001° |
| γ | 65.881 ± 0.001° |
| Cell volume | 3988.1 ± 0.5 Å3 |
| Cell temperature | 193 ± 2 K |
| Ambient diffraction temperature | 193 ± 2 K |
| Number of distinct elements | 7 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0564 |
| Residual factor for observed reflections | 0.0457 |
| Weighted residual factors for the observed reflections | 0.1133 |
| Weighted residual factors for all reflections included in the refinement | 0.1175 |
| Goodness-of-fit parameter for observed reflections | 1.026 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |