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CIF Information Card
Information card for 7015467
7015466 << 7015467 >> 7015468Preview
|
Coordinates |
7015467.cif |
Structure parameters
| Formula | - C54 H108 O13 P Rh Si8 - |
| Calculated formula | - C54 H108 O13 P Rh Si8 - |
| Title of publication | Silsesquioxyl rhodium(I) complexes‒synthesis, structure and catalytic activity. |
| Authors of publication | Marciniec, Bogdan; Kownacki, Ireneusz; Franczyk, Adrian; Kubicki, Maciej |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2011 |
| Journal volume | 40 |
| Journal issue | 18 |
| Pages of publication | 5073 - 5077 |
| a | 10.9023 ± 0.0012 Å |
| b | 14.8954 ± 0.0018 Å |
| c | 21.769 ± 0.003 Å |
| α | 99.731 ± 0.012° |
| β | 98.469 ± 0.009° |
| γ | 104.467 ± 0.01° |
| Cell volume | 3306.6 ± 0.8 Å3 |
| Cell temperature | 100 ± 1 K |
| Ambient diffraction temperature | 100 ± 1 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0958 |
| Residual factor for observed reflections | 0.0563 |
| Weighted residual factors for the observed reflections | 0.1313 |
| Weighted residual factors for all reflections included in the refinement | 0.1368 |
| Goodness-of-fit parameter for observed reflections | 0.96 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |