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CIF Information Card
Information card for 7015634
7015633 << 7015634 >> 7015635Preview
|
Coordinates |
7015634.cif |
Structure parameters
| Formula | - C33 H27 N21 - |
| Calculated formula | - C33 H27 N21 - |
| Title of publication | Synthesis, characterization, crystal structure and preliminary reactivity behaviour of new heteropolytopic ligands based on the 1,3,5-triazine spacer and pyrazolyl, tris-pyrazolylmethyl and tris-pyrazolylethoxy bonding fragments. |
| Authors of publication | Di Nicola, C.; Garau, F.; Marchetti, F.; Monari, M.; Pandolfo, L.; Pettinari, C.; Venzo, A. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2011 |
| Journal volume | 40 |
| Journal issue | 18 |
| Pages of publication | 4941 - 4953 |
| a | 8.8379 ± 0.0005 Å |
| b | 11.6404 ± 0.0007 Å |
| c | 18.3088 ± 0.0011 Å |
| α | 80.857 ± 0.001° |
| β | 85.384 ± 0.001° |
| γ | 67.977 ± 0.001° |
| Cell volume | 1723.48 ± 0.18 Å3 |
| Cell temperature | 273 ± 2 K |
| Ambient diffraction temperature | 273 ± 2 K |
| Number of distinct elements | 3 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.1311 |
| Residual factor for observed reflections | 0.0792 |
| Weighted residual factors for the observed reflections | 0.251 |
| Weighted residual factors for all reflections included in the refinement | 0.291 |
| Goodness-of-fit parameter for observed reflections | 1.059 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |