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CIF Information Card
Information card for 7015691
7015690 << 7015691 >> 7015692Preview
|
Coordinates |
7015691.cif |
Structure parameters
| Formula | - C24 H45 B F4 Ni O P2 - |
| Calculated formula | - C24 H45 B F4 Ni O P2 - |
| Title of publication | Nickel(II) hydride and fluoride pincer complexes and their reactivity with Lewis acids BX3·L (X = H, L = thf; X = F, L = Et2O). |
| Authors of publication | Rossin, Andrea; Peruzzini, Maurizio; Zanobini, Fabrizio |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2011 |
| Journal volume | 40 |
| Journal issue | 17 |
| Pages of publication | 4447 - 4452 |
| a | 17.28 ± 0.008 Å |
| b | 15.826 ± 0.007 Å |
| c | 20.966 ± 0.009 Å |
| α | 90 ± 0.005° |
| β | 90 ± 0.005° |
| γ | 90 ± 0.005° |
| Cell volume | 5734 ± 4 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 7 |
| Hermann-Mauguin symmetry space group | P b c a |
| Hall symmetry space group | -P 2ac 2ab |
| Residual factor for all reflections | 0.0806 |
| Residual factor for observed reflections | 0.0326 |
| Weighted residual factors for the observed reflections | 0.0465 |
| Weighted residual factors for all reflections included in the refinement | 0.0525 |
| Goodness-of-fit parameter for observed reflections | 0.755 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |