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CIF Information Card
Information card for 7015730
7015729 << 7015730 >> 7015731Preview
|
Coordinates |
7015730.cif |
Structure parameters
| Formula | - C27 H36 N6 - |
| Calculated formula | - C27 H36 N6 - |
| Title of publication | Cu(i) catalysed cyclopropanation with enantiopure scorpionate type ligands derived from (+)-camphor or (-)-menthone. |
| Authors of publication | Godau, Tom; Bleifuß, Sascha M; Müller, Astrid L; Roth, Thomas; Hoffmann, Susanne; Heinemann, Frank W.; Burzlaff, Nicolai |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2011 |
| Journal volume | 40 |
| Journal issue | 24 |
| Pages of publication | 6547 - 6554 |
| a | 25.4805 ± 0.0012 Å |
| b | 7.7565 ± 0.0005 Å |
| c | 17.8684 ± 0.0007 Å |
| α | 90° |
| β | 133.701 ± 0.003° |
| γ | 90° |
| Cell volume | 2553.1 ± 0.3 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 3 |
| Hermann-Mauguin symmetry space group | C 1 2 1 |
| Hall symmetry space group | C 2y |
| Residual factor for all reflections | 0.0541 |
| Residual factor for observed reflections | 0.0423 |
| Weighted residual factors for the observed reflections | 0.1074 |
| Weighted residual factors for all reflections included in the refinement | 0.1141 |
| Goodness-of-fit parameter for observed reflections | 1.066 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |