Crystallography Open Database
| COD Home |
|---|
| Accessing COD Data |
|---|
| Add Your Data |
|---|
| Documentation |
|---|
CIF Information Card
Information card for 7015732
7015731 << 7015732 >> 7015733Preview
|
Coordinates |
7015732.cif |
Structure parameters
| Formula | - C27 H40 N6 - |
| Calculated formula | - C27 H40 N6 - |
| Title of publication | Cu(i) catalysed cyclopropanation with enantiopure scorpionate type ligands derived from (+)-camphor or (-)-menthone. |
| Authors of publication | Godau, Tom; Bleifuß, Sascha M; Müller, Astrid L; Roth, Thomas; Hoffmann, Susanne; Heinemann, Frank W.; Burzlaff, Nicolai |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2011 |
| Journal volume | 40 |
| Journal issue | 24 |
| Pages of publication | 6547 - 6554 |
| a | 8.8408 ± 0.0003 Å |
| b | 11.2369 ± 0.0004 Å |
| c | 27.045 ± 0.0009 Å |
| α | 90° |
| β | 93.068 ± 0.002° |
| γ | 90° |
| Cell volume | 2682.89 ± 0.16 Å3 |
| Cell temperature | 230 ± 2 K |
| Ambient diffraction temperature | 230 ± 2 K |
| Number of distinct elements | 3 |
| Hermann-Mauguin symmetry space group | P 1 21 1 |
| Hall symmetry space group | P 2yb |
| Residual factor for all reflections | 0.0753 |
| Residual factor for observed reflections | 0.0533 |
| Weighted residual factors for the observed reflections | 0.1328 |
| Weighted residual factors for all reflections included in the refinement | 0.1485 |
| Goodness-of-fit parameter for observed reflections | 1.021 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |