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CIF Information Card
Information card for 7101622
7101621 << 7101622 >> 7101623Preview
|
Coordinates |
7101622.cif |
Structure parameters
| Formula | - C20 H23 F3 N O4 P Pd S - |
| Calculated formula | - C20 H23 F3 N O4 P Pd S - |
| Title of publication | Structurally characterized intermediates in the stepwise insertion of CO-ethylene or CO-methyl acrylate into the metal-carbon bond of Pd(II) complexes stabilized by (phosphinomethyl)oxazoline ligands. |
| Authors of publication | Agostinho, Magno; Braunstein, Pierre |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 1 |
| Pages of publication | 58 - 60 |
| a | 8.333 ± 0.001 Å |
| b | 9.827 ± 0.002 Å |
| c | 14.261 ± 0.003 Å |
| α | 92.55 ± 0.05° |
| β | 100.18 ± 0.05° |
| γ | 98.93 ± 0.05° |
| Cell volume | 1132.4 ± 0.4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 8 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0388 |
| Residual factor for observed reflections | 0.0303 |
| Weighted residual factors for the observed reflections | 0.0676 |
| Weighted residual factors for all reflections included in the refinement | 0.0714 |
| Goodness-of-fit parameter for observed reflections | 1.054 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |