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CIF Information Card
Information card for 7101623
7101622 << 7101623 >> 7101624Preview
|
Coordinates |
7101623.cif |
Structure parameters
| Formula | - C20 H23 Cl N O2 P Pd - |
| Calculated formula | - C20 H23 Cl N O2 P Pd - |
| Title of publication | Structurally characterized intermediates in the stepwise insertion of CO-ethylene or CO-methyl acrylate into the metal-carbon bond of Pd(II) complexes stabilized by (phosphinomethyl)oxazoline ligands. |
| Authors of publication | Agostinho, Magno; Braunstein, Pierre |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 1 |
| Pages of publication | 58 - 60 |
| a | 8.962 ± 0.005 Å |
| b | 10.1 ± 0.005 Å |
| c | 12.534 ± 0.005 Å |
| α | 82.414 ± 0.005° |
| β | 80.486 ± 0.005° |
| γ | 64.312 ± 0.005° |
| Cell volume | 1006 ± 0.9 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 7 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0246 |
| Residual factor for observed reflections | 0.0226 |
| Weighted residual factors for the observed reflections | 0.0626 |
| Weighted residual factors for all reflections included in the refinement | 0.0635 |
| Goodness-of-fit parameter for observed reflections | 1.046 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |