Crystallography Open Database
| COD Home |
|---|
| Accessing COD Data |
|---|
| Add Your Data |
|---|
| Documentation |
|---|
CIF Information Card
Information card for 7101651
7101650 << 7101651 >> 7101652Preview
|
Coordinates |
7101651.cif |
Structure parameters
| Formula | - C21 H21 F N2 O3 - |
| Calculated formula | - C21 H21 F N2 O3 - |
| Title of publication | The remarkable effect of the 7-substituent in the diastereoselective oxidative rearrangement of indoles: asymmetric synthesis of 3,3-disubstituted oxindoles. |
| Authors of publication | Lachia, Mathilde; Poriel, Cyril; Slawin, Alexandra M Z; Moody, Christopher J |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 3 |
| Pages of publication | 286 - 288 |
| a | 9.797 ± 0.002 Å |
| b | 12.303 ± 0.002 Å |
| c | 14.883 ± 0.003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 1793.9 ± 0.6 Å3 |
| Cell temperature | 93 ± 2 K |
| Ambient diffraction temperature | 93 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P 21 21 21 |
| Hall symmetry space group | P 2ac 2ab |
| Residual factor for all reflections | 0.0414 |
| Residual factor for observed reflections | 0.0369 |
| Weighted residual factors for the observed reflections | 0.0812 |
| Weighted residual factors for all reflections included in the refinement | 0.0837 |
| Goodness-of-fit parameter for observed reflections | 1.085 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |