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CIF Information Card
Information card for 7101668
7101667 << 7101668 >> 7101669Preview
|
Coordinates |
7101668.cif |
Structure parameters
| Formula | - C51 H51 Cl3 O3 P4 Pd - |
| Calculated formula | - C51 H49 Cl3 O3 P4 Pd - |
| Title of publication | Novel route to carbodiphosphoranes producing a new P,C,P pincer carbene ligand. |
| Authors of publication | Stallinger, Silvia; Reitsamer, Christian; Schuh, Walter; Kopacka, Holger; Wurst, Klaus; Peringer, Paul |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 5 |
| Pages of publication | 510 - 512 |
| a | 9.2897 ± 0.0003 Å |
| b | 13.5853 ± 0.0006 Å |
| c | 19.9199 ± 0.0007 Å |
| α | 86.39 ± 0.002° |
| β | 89.649 ± 0.002° |
| γ | 72.822 ± 0.002° |
| Cell volume | 2396.84 ± 0.16 Å3 |
| Cell temperature | 233 ± 2 K |
| Ambient diffraction temperature | 233 ± 2 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0635 |
| Residual factor for observed reflections | 0.042 |
| Weighted residual factors for the observed reflections | 0.0755 |
| Weighted residual factors for all reflections included in the refinement | 0.0813 |
| Goodness-of-fit parameter for observed reflections | 1.039 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |