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CIF Information Card
Information card for 7101716
7101715 << 7101716 >> 7101717Preview
|
Coordinates |
7101716.cif |
Structure parameters
| Formula | - C33 H41 I5 N2 - |
| Calculated formula | - C33 H41 I5 N2 - |
| Title of publication | beta-Diiminato ligand (L) transformations in reactions of KL with PI3 and I2 [L = {N(C6H3Pr(i)2-2,6)C(H)}2CPh]. |
| Authors of publication | Hitchcock, Peter B; Lappert, Michael F; Li, Gang; Protchenko, Andrey V |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 8 |
| Pages of publication | 846 - 848 |
| a | 21.8936 ± 0.0005 Å |
| b | 13.9582 ± 0.0003 Å |
| c | 12.3029 ± 0.0003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3759.71 ± 0.15 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 4 |
| Hermann-Mauguin symmetry space group | P n c 2 |
| Hall symmetry space group | P 2 -2bc |
| Residual factor for all reflections | 0.0554 |
| Residual factor for observed reflections | 0.0393 |
| Weighted residual factors for the observed reflections | 0.0796 |
| Weighted residual factors for all reflections included in the refinement | 0.0854 |
| Goodness-of-fit parameter for observed reflections | 1.02 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |