Crystallography Open Database
| COD Home |
|---|
| Accessing COD Data |
|---|
| Add Your Data |
|---|
| Documentation |
|---|
CIF Information Card
Information card for 7101749
7101748 << 7101749 >> 7101750Preview
|
Coordinates |
7101749.cif |
Structure parameters
| Formula | - C15 H33 Br2 Ni O2 P2 - |
| Calculated formula | - C15 H33 Br2 Ni O2 P2 - |
| Title of publication | New pincer-type diphosphinito (POCOP) complexes of NiII and NiIII. |
| Authors of publication | Pandarus, Valerica; Zargarian, Davit |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 9 |
| Pages of publication | 978 - 980 |
| a | 34.4889 ± 0.0008 Å |
| b | 7.0423 ± 0.0002 Å |
| c | 22.1302 ± 0.0005 Å |
| α | 90° |
| β | 127.664 ± 0.001° |
| γ | 90° |
| Cell volume | 4254.9 ± 0.18 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | C 1 2/c 1 |
| Hall symmetry space group | -C 2yc |
| Residual factor for all reflections | 0.0546 |
| Residual factor for observed reflections | 0.052 |
| Weighted residual factors for the observed reflections | 0.1735 |
| Weighted residual factors for all reflections included in the refinement | 0.1758 |
| Goodness-of-fit parameter for observed reflections | 1.082 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |