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CIF Information Card
Information card for 7101757
7101756 << 7101757 >> 7101758Preview
|
Coordinates |
7101757.cif |
Structure parameters
| Formula | - C108 H257 N15 Na2 Ni16 O89 - |
| Calculated formula | - C108 H209 N15 Na2 Ni16 O89 - |
| Title of publication | A one-pot synthesis of a paramagnetic high-nuclearity nickel(II) cluster: an octadecanuclear Ni(II)16Na(I)2 metal aggregate. |
| Authors of publication | Biswas, Biplab; Khanra, Sumit; Weyhermüller, Thomas; Chaudhuri, Phalguni |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 10 |
| Pages of publication | 1059 - 1061 |
| a | 19.3308 ± 0.0006 Å |
| b | 26.0589 ± 0.0008 Å |
| c | 36.1281 ± 0.0012 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 18199.1 ± 1 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | P 21 21 21 |
| Hall symmetry space group | P 2ac 2ab |
| Residual factor for all reflections | 0.1061 |
| Residual factor for observed reflections | 0.0794 |
| Weighted residual factors for the observed reflections | 0.148 |
| Weighted residual factors for all reflections included in the refinement | 0.1592 |
| Goodness-of-fit parameter for observed reflections | 1.139 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |