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CIF Information Card
Information card for 7101796
7101795 << 7101796 >> 7101797Preview
|
Coordinates |
7101796.cif |
Structure parameters
| Formula | - C72 H114 Cl2 N4 O2 Pd2 - |
| Calculated formula | - C72 H114 Cl2 N4 O2 Pd2 - |
| Title of publication | Synthesis and reactivity of alkyl-palladium N-heterocyclic carbene complexes. |
| Authors of publication | Esposito, Oriana; Lewis, Alexandra K de K; Hitchcock, Peter B; Caddick, Stephen; Cloke, F Geoffrey N |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 11 |
| Pages of publication | 1157 - 1159 |
| a | 22.4708 ± 0.0006 Å |
| b | 17.984 ± 0.0007 Å |
| c | 19.059 ± 0.0005 Å |
| α | 90° |
| β | 106.288 ± 0.002° |
| γ | 90° |
| Cell volume | 7392.9 ± 0.4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | C 1 2/c 1 |
| Hall symmetry space group | -C 2yc |
| Residual factor for all reflections | 0.0681 |
| Residual factor for observed reflections | 0.043 |
| Weighted residual factors for the observed reflections | 0.1037 |
| Weighted residual factors for all reflections included in the refinement | 0.1241 |
| Goodness-of-fit parameter for observed reflections | 0.774 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |