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CIF Information Card
Information card for 7101797
7101796 << 7101797 >> 7101798Preview
|
Coordinates |
7101797.cif |
Structure parameters
| Formula | - C20 H40 Cl N3 O Pd - |
| Calculated formula | - C20 H40 Cl N3 O Pd - |
| Title of publication | Synthesis and reactivity of alkyl-palladium N-heterocyclic carbene complexes. |
| Authors of publication | Esposito, Oriana; Lewis, Alexandra K de K; Hitchcock, Peter B; Caddick, Stephen; Cloke, F Geoffrey N |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 11 |
| Pages of publication | 1157 - 1159 |
| a | 9.6642 ± 0.0003 Å |
| b | 23.1895 ± 0.0005 Å |
| c | 10.4673 ± 0.0003 Å |
| α | 90° |
| β | 95.324 ± 0.001° |
| γ | 90° |
| Cell volume | 2335.69 ± 0.11 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Hermann-Mauguin symmetry space group | P 1 21/n 1 |
| Hall symmetry space group | -P 2yn |
| Residual factor for all reflections | 0.0774 |
| Residual factor for observed reflections | 0.0457 |
| Weighted residual factors for the observed reflections | 0.108 |
| Weighted residual factors for all reflections included in the refinement | 0.1287 |
| Goodness-of-fit parameter for observed reflections | 0.821 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |