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CIF Information Card
Information card for 7101798
7101797 << 7101798 >> 7101799Preview
|
Coordinates |
7101798.cif |
Structure parameters
| Formula | - C21 H21 I N2 O4 - |
| Calculated formula | - C21 H21 I N2 O4 - |
| Title of publication | Reaction of imines with N-iodosuccinimide (NIS): unexpected formation of stable 1 : 1 complexes. |
| Authors of publication | Castellote, Isabel; Morón, María; Burgos, Carolina; Alvarez-Builla, Julio; Martin, Avelino; Gómez-Sal, Pilar; Vaquero, Juan J |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 12 |
| Pages of publication | 1281 - 1283 |
| a | 8.959 ± 0.0002 Å |
| b | 12.0504 ± 0.0004 Å |
| c | 19.2674 ± 0.0011 Å |
| α | 90° |
| β | 96.661 ± 0.004° |
| γ | 90° |
| Cell volume | 2066.06 ± 0.14 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P 1 21/c 1 |
| Hall symmetry space group | -P 2ybc |
| Residual factor for all reflections | 0.0238 |
| Residual factor for observed reflections | 0.0195 |
| Weighted residual factors for the observed reflections | 0.0587 |
| Weighted residual factors for all reflections included in the refinement | 0.0623 |
| Goodness-of-fit parameter for observed reflections | 0.843 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |