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CIF Information Card
Information card for 7101883
7101882 << 7101883 >> 7101884Preview
|
Coordinates |
7101883.cif |
Structure parameters
| Formula | - C38 H66 Cl4 O2 Ru2 - |
| Calculated formula | - C38 H66 Cl4 O2 Ru2 - |
| Title of publication | A new coupling reaction for the synthesis of ruthenium half-sandwich complexes with sterically demanding cyclopentadienyl ligands. |
| Authors of publication | Gauthier, Sébastien; Solari, Euro; Dutta, Barnali; Scopelliti, Rosario; Severin, Kay |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2007 |
| Journal issue | 18 |
| Pages of publication | 1837 - 1839 |
| a | 23.624 ± 0.002 Å |
| b | 14.0305 ± 0.001 Å |
| c | 12.2973 ± 0.0008 Å |
| α | 90° |
| β | 90.572 ± 0.006° |
| γ | 90° |
| Cell volume | 4075.8 ± 0.5 Å3 |
| Cell temperature | 140 ± 2 K |
| Ambient diffraction temperature | 140 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P 1 21/c 1 |
| Hall symmetry space group | -P 2ybc |
| Residual factor for all reflections | 0.0823 |
| Residual factor for observed reflections | 0.0586 |
| Weighted residual factors for the observed reflections | 0.1438 |
| Weighted residual factors for all reflections included in the refinement | 0.1557 |
| Goodness-of-fit parameter for observed reflections | 0.995 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |