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CIF Information Card
Information card for 7151728
7151727 << 7151728 >> 7151729Preview
|
Coordinates |
7151728.cif |
Structure parameters
| Formula | - C37 H52 Cl N O11 - |
| Calculated formula | - C37 H52 Cl N O11 - |
| Title of publication | Highly efficient asymmetric vinylogous Mannich reaction induced by O-pivaloylated d-galactosylamine as the chiral auxiliary. |
| Authors of publication | Yu, Jipan; Miao, Zhiwei; Chen, Ruyu |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 6 |
| Pages of publication | 1756 - 1762 |
| a | 9.772 ± 0.002 Å |
| b | 17.25 ± 0.004 Å |
| c | 11.937 ± 0.002 Å |
| α | 90° |
| β | 97.6 ± 0.03° |
| γ | 90° |
| Cell volume | 1994.5 ± 0.7 Å3 |
| Cell temperature | 113 ± 2 K |
| Ambient diffraction temperature | 113 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P 1 21 1 |
| Hall symmetry space group | P 2yb |
| Residual factor for all reflections | 0.0655 |
| Residual factor for observed reflections | 0.0534 |
| Weighted residual factors for the observed reflections | 0.1276 |
| Weighted residual factors for all reflections included in the refinement | 0.1373 |
| Goodness-of-fit parameter for observed reflections | 1.017 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |