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Information card for entry 7151728
Preview
Coordinates | 7151728.cif |
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Original paper (by DOI) | HTML |
Formula | C37 H52 Cl N O11 |
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Calculated formula | C37 H52 Cl N O11 |
Title of publication | Highly efficient asymmetric vinylogous Mannich reaction induced by O-pivaloylated d-galactosylamine as the chiral auxiliary. |
Authors of publication | Yu, Jipan; Miao, Zhiwei; Chen, Ruyu |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2011 |
Journal volume | 9 |
Journal issue | 6 |
Pages of publication | 1756 - 1762 |
a | 9.772 ± 0.002 Å |
b | 17.25 ± 0.004 Å |
c | 11.937 ± 0.002 Å |
α | 90° |
β | 97.6 ± 0.03° |
γ | 90° |
Cell volume | 1994.5 ± 0.7 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0655 |
Residual factor for significantly intense reflections | 0.0534 |
Weighted residual factors for significantly intense reflections | 0.1276 |
Weighted residual factors for all reflections included in the refinement | 0.1373 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.017 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
180303 (current) | 2016-03-26 | cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/17. |
7151728.cif |
120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7151728.cif |
35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7151728.cif |
15009 | 2011-03-12 | ../uploads/cif-deposit/cod/cif Adding structures of 7151728 via cif-deposit CGI script. |
7151728.cif |
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Users of the data should acknowledge the original authors of the
structural data.