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CIF Information Card
Information card for 7151763
7151762 << 7151763 >> 7151764Preview
|
Coordinates |
7151763.cif |
Structure parameters
| Formula | - C21 H29 N O6 - |
| Calculated formula | - C21 H29 N O6 - |
| Title of publication | Total synthesis of the Amaryllidaceae alkaloid clivonine. |
| Authors of publication | Haning, Helmut; Giró-Mañas, Carles; Paddock, Victoria L.; Bochet, Christian G.; White, Andrew J. P.; Bernardinelli, Gerald; Mann, Inderjit; Oppolzer, Wolfang; Spivey, Alan C. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 8 |
| Pages of publication | 2809 - 2820 |
| a | 7.2818 ± 0.0001 Å |
| b | 33.8728 ± 0.0003 Å |
| c | 8.3252 ± 0.0001 Å |
| α | 90° |
| β | 104.148 ± 0.001° |
| γ | 90° |
| Cell volume | 1991.17 ± 0.04 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 4 |
| Hermann-Mauguin symmetry space group | P 1 21/n 1 |
| Hall symmetry space group | -P 2yn |
| Residual factor for all reflections | 0.0458 |
| Residual factor for observed reflections | 0.0424 |
| Weighted residual factors for the observed reflections | 0.1224 |
| Weighted residual factors for all reflections included in the refinement | 0.1248 |
| Goodness-of-fit parameter for observed reflections | 1.088 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |