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CIF Information Card
Information card for 7151765
7151764 << 7151765 >> 7151766Preview
|
Coordinates |
7151765.cif |
Structure parameters
| Formula | - C25 H26 Cl N O5 - |
| Calculated formula | - C25 H26 Cl N O5 - |
| Title of publication | Total synthesis of the Amaryllidaceae alkaloid clivonine. |
| Authors of publication | Haning, Helmut; Giró-Mañas, Carles; Paddock, Victoria L.; Bochet, Christian G.; White, Andrew J. P.; Bernardinelli, Gerald; Mann, Inderjit; Oppolzer, Wolfang; Spivey, Alan C. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 8 |
| Pages of publication | 2809 - 2820 |
| a | 6.0988 ± 0.0002 Å |
| b | 11.8551 ± 0.0004 Å |
| c | 16.3205 ± 0.0005 Å |
| α | 102.804 ± 0.003° |
| β | 98.74 ± 0.003° |
| γ | 102.13 ± 0.003° |
| Cell volume | 1100.31 ± 0.07 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.0511 |
| Residual factor for observed reflections | 0.0368 |
| Weighted residual factors for the observed reflections | 0.1013 |
| Weighted residual factors for all reflections included in the refinement | 0.1087 |
| Goodness-of-fit parameter for observed reflections | 1.042 |
| Diffraction radiation wavelength | 1.54248 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |