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CIF Information Card
Information card for 7151798
7151797 << 7151798 >> 7151799Preview
|
Coordinates |
7151798.cif |
Structure parameters
| Formula | - C9 H19 N O - |
| Calculated formula | - C9 H19 N O - |
| Title of publication | Anhydrous TEMPO-H: reactions of a good hydrogen atom donor with low-valent carbon centres. |
| Authors of publication | Giffin, Nick A.; Makramalla, Miller; Hendsbee, Arthur D.; Robertson, Katherine N.; Sherren, Cody; Pye, Cory C.; Masuda, Jason D.; Clyburne, Jason A. C. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 10 |
| Pages of publication | 3672 - 3680 |
| a | 18.7761 ± 0.0016 Å |
| b | 18.7761 ± 0.0016 Å |
| c | 43.329 ± 0.004 Å |
| α | 90° |
| β | 90° |
| γ | 120° |
| Cell volume | 13229 ± 2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Hermann-Mauguin symmetry space group | R -3 :H |
| Hall symmetry space group | -R 3 |
| Residual factor for all reflections | 0.0781 |
| Residual factor for observed reflections | 0.042 |
| Weighted residual factors for the observed reflections | 0.0861 |
| Weighted residual factors for all reflections included in the refinement | 0.0993 |
| Goodness-of-fit parameter for observed reflections | 1.096 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |