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CIF Information Card
Information card for 7151812
7151811 << 7151812 >> 7151813Preview
|
Coordinates |
7151812.cif |
Structure parameters
| Formula | - C42 H49 N O3 Si - |
| Calculated formula | - C42 H49 N O3 Si - |
| Title of publication | A stereoselective, Sm(II)-mediated approach to decorated cis-hydrindanes: synthetic studies on faurinone and pleuromutilin. |
| Authors of publication | Findley, Thomas J. K.; Sucunza, David; Miller, Laura C.; Helm, Matthew D.; Helliwell, Madeleine; Davies, David T.; Procter, David J. |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 7 |
| Pages of publication | 2433 - 2451 |
| a | 10.4285 ± 0.0015 Å |
| b | 12.4428 ± 0.0015 Å |
| c | 14.7188 ± 0.0015 Å |
| α | 86.41 ± 0.003° |
| β | 72.131 ± 0.002° |
| γ | 86.886 ± 0.003° |
| Cell volume | 1813 ± 0.4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for all reflections | 0.2302 |
| Residual factor for observed reflections | 0.0756 |
| Weighted residual factors for the observed reflections | 0.1387 |
| Weighted residual factors for all reflections included in the refinement | 0.1795 |
| Goodness-of-fit parameter for observed reflections | 0.775 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |