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CIF Information Card
Information card for 7151813
7151812 << 7151813 >> 7151814Preview
|
Coordinates |
7151813.cif |
Structure parameters
| Formula | - C18 H17 N O - |
| Calculated formula | - C18 H17 N O - |
| Title of publication | Efficient iron-mediated approach to pyrano[3,2-a]carbazole alkaloids‒first total syntheses of O-methylmurrayamine A and 7-methoxymurrayacine, first asymmetric synthesis and assignment of the absolute configuration of (-)-trans-dihydroxygirinimbine. |
| Authors of publication | Gruner, Konstanze K.; Hopfmann, Thomas; Matsumoto, Kazuhiro; Jäger, Anne; Katsuki, Tsutomu; Knölker, Hans-Joachim |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 7 |
| Pages of publication | 2057 - 2061 |
| a | 11.96 ± 0.002 Å |
| b | 16.344 ± 0.003 Å |
| c | 7.655 ± 0.002 Å |
| α | 90° |
| β | 109.03 ± 0.03° |
| γ | 90° |
| Cell volume | 1414.6 ± 0.6 Å3 |
| Cell temperature | 198 ± 2 K |
| Ambient diffraction temperature | 198 ± 2 K |
| Number of distinct elements | 4 |
| Hermann-Mauguin symmetry space group | C 1 c 1 |
| Hall symmetry space group | C -2yc |
| Residual factor for all reflections | 0.0593 |
| Residual factor for observed reflections | 0.0375 |
| Weighted residual factors for the observed reflections | 0.0747 |
| Weighted residual factors for all reflections included in the refinement | 0.0811 |
| Goodness-of-fit parameter for observed reflections | 1.037 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |