Crystallography Open Database
| COD Home |
|---|
| Accessing COD Data |
|---|
| Add Your Data |
|---|
| Documentation |
|---|
CIF Information Card
Information card for 7151831
7151830 << 7151831 >> 7151832Preview
|
Coordinates |
7151831.cif |
Structure parameters
| Formula | - C27 H17 Cl2 N Se2 - |
| Calculated formula | - C27 H17 Cl2 N Se2 - |
| Title of publication | Photochemical intramolecular cyclization of o-alkynylaryl isocyanides with organic dichalcogenides leading to 2,4-bischalcogenated quinolines. |
| Authors of publication | Mitamura, Takenori; Iwata, Kimiyo; Nomoto, Akihiro; Ogawa, Akiya |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2011 |
| Journal volume | 9 |
| Journal issue | 10 |
| Pages of publication | 3768 - 3775 |
| a | 6.0736 ± 0.0003 Å |
| b | 11.6934 ± 0.0005 Å |
| c | 17.749 ± 0.0009 Å |
| α | 74.4693 ± 0.0012° |
| β | 86.7204 ± 0.0013° |
| γ | 73.3481 ± 0.0013° |
| Cell volume | 1163.33 ± 0.1 Å3 |
| Cell temperature | 103.1 K |
| Ambient diffraction temperature | 103.1 K |
| Number of distinct elements | 5 |
| Hermann-Mauguin symmetry space group | P -1 |
| Hall symmetry space group | -P 1 |
| Residual factor for observed reflections | 0.0582 |
| Weighted residual factors for all reflections included in the refinement | 0.1941 |
| Goodness-of-fit parameter for observed reflections | 1.005 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |