Crystallography Open Database

Information card for entry 1504882

Preview

Coordinates	1504882.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H37 Cl2 O8 Rh2
Calculated formula	C28 H28 Cl2 O8 Rh2
Title of publication	Highly practical catalytic asymmetric 1,4-addition of arylboronic acids in water using new hydrophilic chiral bicyclo[3.3.0] diene ligands.
Authors of publication	Feng, Chen-Guo; Wang, Zhi-Qian; Shao, Cheng; Xu, Ming-Hua; Lin, Guo-Qiang
Journal of publication	Organic letters
Year of publication	2008
Journal volume	10
Journal issue	18
Pages of publication	4101 - 4104
a	9.7534 ± 0.001 Å
b	9.9312 ± 0.001 Å
c	28.882 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	2797.6 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0501
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.1192
Weighted residual factors for all reflections included in the refinement	0.1206
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1504882.cif
91932	2013-12-28	cif/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the range 1 CIFs.	1504882.cif
42432	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 1504882 via cif-deposit CGI script.	1504882.cif