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Information card for entry 1504893
Preview
| Coordinates | 1504893.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | ChemSpider |
| Formula | C24 H27 N O6 |
|---|---|
| Calculated formula | C24 H27 N O6 |
| SMILES | O(C(=O)CN1C(=O)c2c([C@H](C(=O)O)[C@H]1[C@@H](OCc1ccccc1)C(C)C)cccc2)C |
| Title of publication | Trans-stereoselectivity in the reaction between homophthalic anhydride and imines. |
| Authors of publication | Vara, Yosu; Bello, Tamara; Aldaba, Eneko; Arrieta, Ana; Pizarro, José L; Arriortua, María I; Lopez, Xabier; Cossío, Fernando P |
| Journal of publication | Organic letters |
| Year of publication | 2008 |
| Journal volume | 10 |
| Journal issue | 21 |
| Pages of publication | 4759 - 4762 |
| a | 11.0148 ± 0.0004 Å |
| b | 15.6616 ± 0.0007 Å |
| c | 13.2742 ± 0.0005 Å |
| α | 90° |
| β | 91.291 ± 0.003° |
| γ | 90° |
| Cell volume | 2289.34 ± 0.16 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0579 |
| Residual factor for significantly intense reflections | 0.0362 |
| Weighted residual factors for significantly intense reflections | 0.0712 |
| Weighted residual factors for all reflections included in the refinement | 0.0765 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.887 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 201954 (current) | 2017-10-13 | cif/ Marking COD entries in range 1 that are known to be related to ChemSpider entries using the _cod_related_entry data loop. |
1504893.cif |
| 176729 | 2016-02-18 | cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1. |
1504893.cif |
| 91932 | 2013-12-28 | cif/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the range 1 CIFs. |
1504893.cif |
| 42440 | 2012-03-13 | ../uploads/cif-deposit/cod/cif Adding structures of 1504890, 1504891, 1504892, 1504893 via cif-deposit CGI script. |
1504893.cif |
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Users of the data should acknowledge the original authors of the
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