Crystallography Open Database

Information card for entry 1508071

Preview

Coordinates	1508071.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H40 N4 U
Calculated formula	C32 H25 N4 U
Title of publication	Uranium azide photolysis results in C-H bond activation and provides evidence for a terminal uranium nitride.
Authors of publication	Thomson, Robert K.; Cantat, Thibault; Scott, Brian L.; Morris, David E.; Batista, Enrique R.; Kiplinger, Jaqueline L.
Journal of publication	Nature chemistry
Year of publication	2010
Journal volume	2
Journal issue	9
Pages of publication	723 - 729
a	17.482 ± 0.004 Å
b	12.657 ± 0.003 Å
c	12.915 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	2857.7 ± 1.2 Å³
Cell temperature	120 ± 1 K
Ambient diffraction temperature	120 ± 1 K
Number of distinct elements	4
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0736
Residual factor for significantly intense reflections	0.0568
Weighted residual factors for significantly intense reflections	0.1599
Weighted residual factors for all reflections included in the refinement	0.1625
Goodness-of-fit parameter for all reflections included in the refinement	2.211
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1508071.cif
120071	2014-07-11	Adding DOIs to range 1 structures.	1508071.cif
62617	2012-07-09	cif/ Adding structures of 1508071 via cif-deposit CGI script.	1508071.cif