Crystallography Open Database

Information card for entry 1543102

Preview

Coordinates	1543102.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H72 O Si3 U
Calculated formula	C39 H72 O Si3 U
Title of publication	Steric control of redox events in organo-uranium chemistry: synthesis and characterisation of U(v) oxo and nitrido complexes
Authors of publication	Tsoureas, Nikolaos; Kilpatrick, Alexander F. R.; Inman, Christopher J.; Cloke, F. Geoffrey N.
Journal of publication	Chem. Sci.
Year of publication	2016
Journal volume	7
Journal issue	7
Pages of publication	4624
a	16.6069 ± 0.0013 Å
b	22.4849 ± 0.0019 Å
c	11.2503 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	4200.9 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.1465
Residual factor for significantly intense reflections	0.0983
Weighted residual factors for significantly intense reflections	0.2378
Weighted residual factors for all reflections included in the refinement	0.2983
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
185121 (current)	2016-08-07	cif/ Updating files of 1543100, 1543101, 1543102, 1543103, 1543104, 1543105 Original log message: Adding full bibliography for 1543100--1543105.cif.	1543102.cif
182057	2016-04-13	cif/ Adding structures of 1543100, 1543101, 1543102, 1543103, 1543104, 1543105 via cif-deposit CGI script.	1543102.cif