Crystallography Open Database

Information card for entry 1544648

Preview

Coordinates	1544648.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Dimesityldistibine
Formula	C18 H24 Sb2
Calculated formula	C18 H24 Sb2
Title of publication	Antimony-ligated dysprosium single-molecule magnets as catalysts for stibine dehydrocoupling.
Authors of publication	Pugh, Thomas; Chilton, Nicholas F.; Layfield, Richard A.
Journal of publication	Chemical science
Year of publication	2017
Journal volume	8
Journal issue	3
Pages of publication	2073 - 2080
a	5.174 ± 0.0002 Å
b	7.9835 ± 0.0004 Å
c	11.2694 ± 0.0005 Å
α	88.921 ± 0.004°
β	79.679 ± 0.004°
γ	73.714 ± 0.004°
Cell volume	439.35 ± 0.04 Å³
Cell temperature	150.01 ± 0.13 K
Ambient diffraction temperature	150.01 ± 0.13 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0308
Residual factor for significantly intense reflections	0.0236
Weighted residual factors for significantly intense reflections	0.0516
Weighted residual factors for all reflections included in the refinement	0.0548
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
196364 (current)	2017-05-06	cif/ Updating files of 1544644, 1544645, 1544646, 1544647, 1544648 Original log message: Adding full bibliography for 1544644--1544648.cif.	1544648.cif
193740	2017-03-05	cif/ Updating files of 1544644, 1544645, 1544646, 1544647, 1544648 Original log message: Adding full bibliography for 1544644--1544648.cif.	1544648.cif
188617	2016-11-22	cif/ Adding structures of 1544644, 1544645, 1544646, 1544647, 1544648 via cif-deposit CGI script.	1544648.cif