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Information card for entry 1545188
Preview
| Coordinates | 1545188.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C35 H30 Cl3 N2 O3 P S |
|---|---|
| Calculated formula | C35 H30 Cl3 N2 O3 P S |
| Title of publication | Copper-Catalyzed P-H Insertions of α-Imino Carbenes for the Preparation of 3-Phosphinoylindoles. |
| Authors of publication | Wang, Lisheng; Wu, Yi; Liu, Yang; Yang, Hua; Liu, Xu; Wang, Jianyi; Li, Xiaoxun; Jiang, Jun |
| Journal of publication | Organic letters |
| Year of publication | 2017 |
| Journal volume | 19 |
| Journal issue | 4 |
| Pages of publication | 782 - 785 |
| a | 32.921 ± 0.007 Å |
| b | 11.658 ± 0.002 Å |
| c | 20.29 ± 0.004 Å |
| α | 90° |
| β | 118.58 ± 0.03° |
| γ | 90° |
| Cell volume | 6838 ± 3 Å3 |
| Cell temperature | 293 K |
| Ambient diffraction temperature | 293 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.1042 |
| Residual factor for significantly intense reflections | 0.061 |
| Weighted residual factors for significantly intense reflections | 0.1582 |
| Weighted residual factors for all reflections included in the refinement | 0.1836 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 193648 (current) | 2017-03-04 | cif/ Updating files of 1545188 Original log message: Adding full bibliography for 1545188.cif. |
1545188.cif |
| 191198 | 2017-02-02 | cif/ Adding structures of 1545188 via cif-deposit CGI script. |
1545188.cif |
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Users of the data should acknowledge the original authors of the
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