Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1550229
Preview
| Coordinates | 1550229.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C59 H99 In2 K2 N4 O2 Si4 |
|---|---|
| Calculated formula | C59 H99 In2 K2 N4 O2 Si4 |
| Title of publication | Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds |
| Authors of publication | Anker, Mathew; Lein, Matthias; Coles, Martyn P. |
| Journal of publication | Chemical Science |
| Year of publication | 2019 |
| a | 23.2852 ± 0.0003 Å |
| b | 17.27697 ± 0.00018 Å |
| c | 36.472 ± 0.0005 Å |
| α | 90° |
| β | 108.506 ± 0.0014° |
| γ | 90° |
| Cell volume | 13913.9 ± 0.3 Å3 |
| Cell temperature | 120 ± 0.1 K |
| Ambient diffraction temperature | 120 ± 0.1 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | I 1 2/a 1 |
| Hall space group symbol | -I 2ya |
| Residual factor for all reflections | 0.0464 |
| Residual factor for significantly intense reflections | 0.0426 |
| Weighted residual factors for significantly intense reflections | 0.1034 |
| Weighted residual factors for all reflections included in the refinement | 0.1065 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.081 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 211906 (current) | 2018-11-13 | cif/ Adding structures of 1550224, 1550225, 1550226, 1550227, 1550228, 1550229, 1550230, 1550231, 1550232, 1550233, 1550234, 1550235 via cif-deposit CGI script. |
1550229.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.