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Information card for entry 1550546
Preview
| Coordinates | 1550546.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C93 H114 B2 Cd2 N6 Si2 |
|---|---|
| Calculated formula | C93 H114 B2 Cd2 N6 Si2 |
| Title of publication | Acyclic 1,2-Dimagnesioethanes/-ethene Derived from Magnesium(I) Compounds: Multipurpose Reagents for Organometallic Synthesis |
| Authors of publication | Jones, Cameron; Dange, Deepak; Gair, Andrew; Jones, Dafydd; Juckel, Martin; Aldridge, Simon |
| Journal of publication | Chemical Science |
| Year of publication | 2019 |
| a | 14.733 ± 0.003 Å |
| b | 27.815 ± 0.006 Å |
| c | 11.021 ± 0.002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 4516.4 ± 1.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 18 |
| Hermann-Mauguin space group symbol | P 21 21 2 |
| Hall space group symbol | P 2 2ab |
| Residual factor for all reflections | 0.045 |
| Residual factor for significantly intense reflections | 0.0424 |
| Weighted residual factors for significantly intense reflections | 0.1101 |
| Weighted residual factors for all reflections included in the refinement | 0.1119 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.123 |
| Diffraction radiation wavelength | 0.7109 Å |
| Diffraction radiation type | Synchrotron |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 213486 (current) | 2019-02-05 | cif/ Adding structures of 1550544, 1550545, 1550546, 1550547, 1550548, 1550549, 1550550, 1550551, 1550552, 1550553, 1550554 via cif-deposit CGI script. |
1550546.cif |
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Users of the data should acknowledge the original authors of the
structural data.