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Information card for entry 1550553
Preview
| Coordinates | 1550553.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C74 H98 Ge Mg N3 Si |
|---|---|
| Calculated formula | C74 H98 Ge Mg N3 Si |
| Title of publication | Acyclic 1,2-Dimagnesioethanes/-ethene Derived from Magnesium(I) Compounds: Multipurpose Reagents for Organometallic Synthesis |
| Authors of publication | Jones, Cameron; Dange, Deepak; Gair, Andrew; Jones, Dafydd; Juckel, Martin; Aldridge, Simon |
| Journal of publication | Chemical Science |
| Year of publication | 2019 |
| a | 11.053 ± 0.0007 Å |
| b | 12.9063 ± 0.0009 Å |
| c | 23.4106 ± 0.0016 Å |
| α | 99.68 ± 0.006° |
| β | 97.495 ± 0.006° |
| γ | 95.233 ± 0.005° |
| Cell volume | 3242 ± 0.4 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1057 |
| Residual factor for significantly intense reflections | 0.0748 |
| Weighted residual factors for significantly intense reflections | 0.1753 |
| Weighted residual factors for all reflections included in the refinement | 0.1982 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 213486 (current) | 2019-02-05 | cif/ Adding structures of 1550544, 1550545, 1550546, 1550547, 1550548, 1550549, 1550550, 1550551, 1550552, 1550553, 1550554 via cif-deposit CGI script. |
1550553.cif |
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Users of the data should acknowledge the original authors of the
structural data.