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Information card for entry 1557370
Preview
| Coordinates | 1557370.cif |
|---|---|
| Structure factors | 1557370.hkl |
| Original IUCr paper | HTML |
| Chemical name | 6-[(<i>tert</i>-Butyldimethylsilyl)oxy]-3-ethenyl-7-methoxy-4-[(trimethylsilyl)ethynyl]naphtho[2,3-<i>c</i>]furan-1(3<i>H</i>)-one |
|---|---|
| Formula | C26 H34 O4 Si2 |
| Calculated formula | C26 H34 O4 Si2 |
| Title of publication | 6-[(<i>tert</i>-Butyldimethylsilyl)oxy]-3-ethenyl-7-methoxy-4-[(trimethylsilyl)ethynyl]naphtho[2,3-<i>c</i>]furan-1(3<i>H</i>)-one |
| Authors of publication | Weil, Matthias; Kremsmayr, Thomas; Mihovilovic, Marko D. |
| Journal of publication | IUCrData |
| Year of publication | 2020 |
| Journal volume | 5 |
| Journal issue | 2 |
| Pages of publication | x200224 |
| a | 10.2628 ± 0.0006 Å |
| b | 20.5653 ± 0.0013 Å |
| c | 13.3923 ± 0.0008 Å |
| α | 90° |
| β | 111.638 ± 0.0015° |
| γ | 90° |
| Cell volume | 2627.4 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0591 |
| Residual factor for significantly intense reflections | 0.0408 |
| Weighted residual factors for significantly intense reflections | 0.0955 |
| Weighted residual factors for all reflections included in the refinement | 0.1042 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 248402 (current) | 2020-02-22 | cif/ hkl/ Adding structures of 1557370 via cif-deposit CGI script. |
1557370.cif 1557370.hkl |
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Users of the data should acknowledge the original authors of the
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