Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1560274
Preview
| Coordinates | 1560274.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H40 K N O6 |
|---|---|
| Calculated formula | C32 H40 K N O6 |
| Title of publication | Synthesis of an elusive, stable 2-azaallyl radical guided by electrochemical and reactivity studies of 2-azaallyl anions |
| Authors of publication | Panetti, Grace B.; Carroll, Patrick J.; Gau, Michael R.; Manor, Brian C.; Schelter, Eric J.; Walsh, Patrick J. |
| Journal of publication | Chemical Science |
| Year of publication | 2021 |
| Journal volume | 12 |
| Journal issue | 12 |
| Pages of publication | 4405 - 4410 |
| a | 9.4575 ± 0.0006 Å |
| b | 13.1739 ± 0.0008 Å |
| c | 12.1272 ± 0.0007 Å |
| α | 90° |
| β | 101.138 ± 0.002° |
| γ | 90° |
| Cell volume | 1482.49 ± 0.16 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0239 |
| Residual factor for significantly intense reflections | 0.0231 |
| Weighted residual factors for significantly intense reflections | 0.0581 |
| Weighted residual factors for all reflections included in the refinement | 0.0587 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 263715 (current) | 2021-04-05 | cif/ Updating files of 1560274, 1560275, 1560276, 1560277, 1560278 Original log message: Adding full bibliography for 1560274--1560278.cif. |
1560274.cif |
| 261782 | 2021-02-05 | cif/ Adding structures of 1560274, 1560275, 1560276, 1560277, 1560278 via cif-deposit CGI script. |
1560274.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.