Crystallography Open Database

Information card for entry 1563582

Preview

Coordinates	1563582.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H48 Ce4 N4 O74 Si W12
Calculated formula	C28 H12 Ce4 N4 O74 Si W12
Title of publication	Syntheses, structures and properties of 3D inorganic‒organic hybrid frameworks constructed from lanthanide polymer and Keggin-type tungstosilicate
Authors of publication	Gao, Yuanzhe; Xu, Yanqing; Han, Zhangang; Li, Chunhong; Cui, Fengyun; Chi, Yingnan; Hu, Changwen
Journal of publication	Journal of Solid State Chemistry
Year of publication	2010
Journal volume	183
Journal issue	5
Pages of publication	1000 - 1006
a	11.7554 ± 0.0013 Å
b	14.4359 ± 0.0016 Å
c	14.6933 ± 0.0017 Å
α	111.146 ± 0.002°
β	112.698 ± 0.002°
γ	93.215 ± 0.001°
Cell volume	2089.5 ± 0.4 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2017
Residual factor for significantly intense reflections	0.1202
Weighted residual factors for significantly intense reflections	0.2915
Weighted residual factors for all reflections included in the refinement	0.3379
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
266564 (current)	2021-06-18	cif/ Adding structures of 1563582, 1563583, 1563584, 1563585 via cif-deposit CGI script.	1563582.cif