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Information card for entry 1566532
Preview
| Coordinates | 1566532.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C78 H119 F3 Ga2 N7 Sb2 |
|---|---|
| Calculated formula | C78 H119 F3 Ga2 N7 Sb2 |
| Title of publication | Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides |
| Authors of publication | Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan |
| Journal of publication | Chemical Science |
| Year of publication | 2022 |
| a | 12.1758 ± 0.001 Å |
| b | 27.211 ± 0.002 Å |
| c | 24.248 ± 0.002 Å |
| α | 90° |
| β | 99.805 ± 0.003° |
| γ | 90° |
| Cell volume | 7916.4 ± 1.1 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0398 |
| Residual factor for significantly intense reflections | 0.0322 |
| Weighted residual factors for significantly intense reflections | 0.0824 |
| Weighted residual factors for all reflections included in the refinement | 0.0893 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273286 (current) | 2022-03-04 | cif/ Adding structures of 1566524, 1566525, 1566526, 1566527, 1566528, 1566529, 1566530, 1566531, 1566532, 1566533, 1566534, 1566535, 1566536 via cif-deposit CGI script. |
1566532.cif |
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Users of the data should acknowledge the original authors of the
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