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Information card for entry 1568381
Preview
| Coordinates | 1568381.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C34 H26 Cl N O2 |
|---|---|
| Calculated formula | C34 H26 Cl N O2 |
| Title of publication | Enantioselective direct Michael addition of cyanohydrin ether derivatives to enones catalyzed by chiral bis(guanidino)iminophosphorane organosuperbase. |
| Authors of publication | Das, Saikat; Kondoh, Azusa; Terada, Masahiro |
| Journal of publication | Chemical science |
| Year of publication | 2023 |
| Journal volume | 14 |
| Journal issue | 12 |
| Pages of publication | 3154 - 3159 |
| a | 7.2214 ± 0.0005 Å |
| b | 28.506 ± 0.002 Å |
| c | 13.0812 ± 0.0009 Å |
| α | 90° |
| β | 92.638 ± 0.003° |
| γ | 90° |
| Cell volume | 2690 ± 0.3 Å3 |
| Cell temperature | 100 ± 0.5 K |
| Ambient diffraction temperature | 100 ± 0.5 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0705 |
| Residual factor for significantly intense reflections | 0.0681 |
| Weighted residual factors for significantly intense reflections | 0.1756 |
| Weighted residual factors for all reflections included in the refinement | 0.1777 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.073 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 282305 (current) | 2023-04-04 | cif/ Updating files of 1568381 Original log message: Adding full bibliography for 1568381.cif. |
1568381.cif |
| 280710 | 2023-02-01 | cif/ Adding structures of 1568381 via cif-deposit CGI script. |
1568381.cif |
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