Crystallography Open Database

Information card for entry 1568626

Preview

Coordinates	1568626.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H20 Co O5 P2
Calculated formula	C27 H20 Co O5 P2
Title of publication	An improved cobalt-catalysed alkoxycarbonylation of olefins using secondary phosphine oxide promotors
Authors of publication	Huang, Weiheng; Jackstell, Ralf; Spannenberg, Anke; Beller, Matthias
Journal of publication	Catalysis Science & Technology
Year of publication	2023
Journal volume	13
Journal issue	8
Pages of publication	2475 - 2479
a	41.7016 ± 0.0013 Å
b	15.1215 ± 0.0005 Å
c	19.8592 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	12523 ± 0.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0502
Weighted residual factors for significantly intense reflections	0.1279
Weighted residual factors for all reflections included in the refinement	0.1317
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283006 (current)	2023-05-05	cif/ Updating files of 1568626 Original log message: Adding full bibliography for 1568626.cif.	1568626.cif
281814	2023-03-11	cif/ Adding structures of 1568626 via cif-deposit CGI script.	1568626.cif