Crystallography Open Database

Information card for entry 1568644

Preview

Coordinates	1568644.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H57 N2 P3
Calculated formula	C51 H57 N2 P3
Title of publication	Probing the donor strength of yldiide ligands: synthesis, structure and reactivity of rhodium complexes with a PC<sub>ylide</sub>N pincer ligand.
Authors of publication	Lapointe, Sébastien; Duari, Prakash; Gessner, Viktoria H.
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	14
Pages of publication	3816 - 3825
a	9.724 ± 0.0001 Å
b	22.5867 ± 0.0001 Å
c	10.3002 ± 0.0001 Å
α	90°
β	106.207 ± 0.001°
γ	90°
Cell volume	2172.36 ± 0.03 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0354
Residual factor for significantly intense reflections	0.0343
Weighted residual factors for significantly intense reflections	0.0878
Weighted residual factors for all reflections included in the refinement	0.0889
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	1.54184 Å
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
283173 (current)	2023-05-05	cif/ Updating files of 1568644, 1568645, 1568646, 1568647, 1568648, 1568649, 1568650, 1568651, 1568652, 1568653 Original log message: Adding full bibliography for 1568644--1568653.cif.	1568644.cif
281849	2023-03-14	cif/ Adding structures of 1568644, 1568645, 1568646, 1568647, 1568648, 1568649, 1568650, 1568651, 1568652, 1568653 via cif-deposit CGI script.	1568644.cif