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Information card for entry 1568741
Preview
| Coordinates | 1568741.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C34 H45 B Si2 |
|---|---|
| Calculated formula | C34 H45 B Si2 |
| Title of publication | A donor-supported silavinylidene and silylium ylides: boroles as a flexible platform for versatile Si(ii) chemistry. |
| Authors of publication | Sarcevic, Julijan; Heitkemper, Tobias; Ruth, Paul Niklas; Naß, Leonard; Kubis, Maximilian; Stalke, Dietmar; Sindlinger, Christian P. |
| Journal of publication | Chemical science |
| Year of publication | 2023 |
| Journal volume | 14 |
| Journal issue | 19 |
| Pages of publication | 5148 - 5159 |
| a | 8.7268 ± 0.0004 Å |
| b | 11.9752 ± 0.0005 Å |
| c | 16.8842 ± 0.0008 Å |
| α | 72.238 ± 0.002° |
| β | 79.568 ± 0.002° |
| γ | 73.411 ± 0.002° |
| Cell volume | 1601.88 ± 0.13 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0437 |
| Residual factor for significantly intense reflections | 0.0419 |
| Weighted residual factors for significantly intense reflections | 0.1174 |
| Weighted residual factors for all reflections included in the refinement | 0.1191 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 284214 (current) | 2023-06-05 | cif/ Updating files of 1568738, 1568739, 1568740, 1568741, 1568742, 1568743, 1568744, 1568745, 1568746, 1568747, 1568748, 1568749 Original log message: Adding full bibliography for 1568738--1568749.cif. |
1568741.cif |
| 282161 | 2023-04-01 | cif/ Adding structures of 1568738, 1568739, 1568740, 1568741, 1568742, 1568743, 1568744, 1568745, 1568746, 1568747, 1568748, 1568749 via cif-deposit CGI script. |
1568741.cif |
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public domain and licensed under the
CC0
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Users of the data should acknowledge the original authors of the
structural data.