Crystallography Open Database

Information card for entry 1573557

Preview

Coordinates	1573557.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C67 H99 Dy2 N4
Calculated formula	C67 H99 Dy2 N4
Title of publication	Rare earth benzene tetraanion-bridged amidinate complexes.
Authors of publication	Jin, Peng-Bo; Luo, Qian-Cheng; Gransbury, Gemma K.; Winpenny, Richard E. P.; Mills, David P.; Zheng, Yan-Zhen
Journal of publication	Chemical science
Year of publication	2025
Journal volume	16
Journal issue	4
Pages of publication	1907 - 1924
a	10.8382 ± 0.0001 Å
b	38.9439 ± 0.0005 Å
c	15.0078 ± 0.0003 Å
α	90°
β	105.063 ± 0.002°
γ	90°
Cell volume	6116.87 ± 0.17 Å³
Cell temperature	100 ± 0.7 K
Ambient diffraction temperature	100 ± 0.7 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0855
Residual factor for significantly intense reflections	0.0822
Weighted residual factors for significantly intense reflections	0.2224
Weighted residual factors for all reflections included in the refinement	0.2241
Goodness-of-fit parameter for all reflections included in the refinement	1.134
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
298113 (current)	2025-03-04	cif/ Updating files of 1573553, 1573554, 1573555, 1573556, 1573557, 1573558, 1573559, 1573560, 1573561 Original log message: Adding full bibliography for 1573553--1573561.cif.	1573557.cif
297004	2025-01-01	cif/ Adding structures of 1573553, 1573554, 1573555, 1573556, 1573557, 1573558, 1573559, 1573560, 1573561 via cif-deposit CGI script.	1573557.cif